Surface Roughness and Color Stability of 3D-Printed Denture Base Materials after Simulated Brushing and Thermocycling


Çakmak G., Molinero-Mourelle P., Silva De Paula M., Akay C., Rodriguez Cuellar A., Dönmez M. B., ...More

MATERIALS, vol.15, no.18, 2022 (SCI-Expanded, Scopus) identifier identifier identifier

  • Publication Type: Article / Article
  • Volume: 15 Issue: 18
  • Publication Date: 2022
  • Doi Number: 10.3390/ma15186441
  • Journal Name: MATERIALS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Academic Search Premier, Aerospace Database, CAB Abstracts, Communication Abstracts, Compendex, INSPEC, Metadex, Veterinary Science Database, Directory of Open Access Journals, Civil Engineering Abstracts
  • Keywords: 3D printing, color stability, denture base, surface roughness, thermocycling, FLEXURAL STRENGTH, CAD/CAM, DISINFECTION, ABRASION, HARDNESS, STORAGE
  • Eskisehir Osmangazi University Affiliated: Yes

Abstract

Three-dimensional (3D) printing is increasingly used to fabricate denture base materials. However, information on the effect of simulated brushing and thermocycling on the surface roughness and color stability of 3D-printed denture base materials is lacking. The aim of this study was to evaluate the effect of brushing and thermocycling on the surface roughness and color stability of 3D-printed denture base materials and to compare with those of milled and heat-polymerized denture base resins. Disk-shaped specimens (o 10 mm x 2 mm) were prepared from 4 different denture base resins (NextDent Denture 3D+ (ND); Denturetec (SC); Polident d.o.o (PD); Promolux (CNV)) (n = 10). Surface roughness (R-a) values were measured before and after polishing with a profilometer. Initial color coordinates were measured by using a spectrophotometer after polishing. Specimens were then consecutively subjected to simulated brushing (10,000 cycles), thermocycling (10,000 cycles), and brushing (10,000 cycles) again. R-a and color coordinates were measured after each interval. Color differences (Delta E-00) between each interval were calculated and these values were further evaluated considering previously reported perceptibility (1.72 units) and acceptability (4.08 units) thresholds. Data were analyzed with Friedman, Kruskal-Wallis, and Mann-Whitney U tests (alpha = 0.05). R-a (p >= 0.051) and Delta E-00 (p >= 0.061) values among different time intervals within each material were similar. Within each time interval, significant differences in R-a (p <= 0.002) and Delta E-00 values (p <= 0.001) were observed among materials. Polishing, brushing, and thermocycling resulted in acceptable surface roughness for all materials that were either similar to or below 0.2 mu m. Color of ND printed resin was affected by brushing and thermocycling. All materials had acceptable color stability when reported thresholds are considered.